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Please use this identifier to cite or link to this item: http://repository.iitr.ac.in/handle/123456789/3353
Title: N-(9,9-Dipropyl-9H-fluoren-2-yl)-7-(piperidin-1-yl)-2,1, 3-benzothiadiazol-4-amine
Authors: Bolisetty M.N.K.P.
Justin Thomas, K. R.
Ng S.W.
Tiekink E.R.T.
Published in: Acta Crystallographica Section E: Structure Reports Online
Abstract: In the title compound, C 30H 34N 4S, each of the benzothia-diazole and fluorene fused ring systems is almost planar (r.m.s. deviations = 0.010 and 0.013 Ã…, respectively) and they are inclined to each other with a dihedral angle of 61.69 (3)°; the S atom is directed away from the rest of the molecule. Each of the benzothiadiazole ring N atoms forms a significant intramolecular contact, i.e. N - H⋯N or C - H⋯N. In the crystal, linear supra-molecular chains along the c axis are generated by C - H⋯N interactions involving the tertiary amine N atom.
Citation: Acta Crystallographica Section E: Structure Reports Online (2012), 68(3): o911-o912
URI: https://doi.org/10.1107/S1600536812008239
http://repository.iitr.ac.in/handle/123456789/3353
Issue Date: 2012
Keywords: data-to-parameter ratio = 17.1
mean σ(C-C) = 0.002 Å
R factor = 0.038
single-crystal X-ray study
T = 100 K
wR factor = 0.106
ISSN: 16005368
Author Scopus IDs: 55069391900
57203389297
55548511500
55738821800
Author Affiliations: Bolisetty, M.N.K.P., Organic Materials Laboratory, Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee 247 667, India
Thomas, K.R.J., Organic Materials Laboratory, Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee 247 667, India
Ng, S.W., Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia, Chemistry Department, Faculty of Science, King Abdulaziz University, PO Box 80203, Jeddah, Saudi Arabia
Tiekink, E.R.T., Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia
Corresponding Author: Tiekink, E.R.T.; Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia; email: edward.tiekink@gmail.com
Appears in Collections:Journal Publications [CY]

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