http://repository.iitr.ac.in/handle/123456789/20860| Title: | MCM-41-supported palladium (II) α-diimine complex: A recyclable catalyst for Suzuki-Miyaura coupling reaction |
| Authors: | Sharma S. Singh, Udai Pratap |
| Published in: | Results in Chemistry |
| Abstract: | A MCM-41-supported palladium (II) α-diimine complex has been synthesized via anchoring of 3-chloropropyltriethoxysilane on mesoporous silica MCM-41, followed by grafting α-diimine ligand through the covalent approach to bind with Pd(II) ion. Different analytical technique such FT-IR, TGA, low angle powder XRD, SEM, TEM, ICP-MS and N2 sorption were used to characterize the complex. The complex serves as a highly active and recyclable catalyst for Suzuki-Miyaura coupling reaction affording a variety of biaryls with good yields. © 2021 The Author(s) |
| Citation: | Results in Chemistry, 3 |
| URI: | https://doi.org/10.1016/j.rechem.2021.100189 http://repository.iitr.ac.in/handle/123456789/20860 |
| Issue Date: | 2021 |
| Publisher: | Elsevier B.V. |
| Keywords: | Aryl halide Catalyst MCM-41 Mesoporous material Palladium (II) complex Phenylboronic acid |
| ISSN: | 22117156 |
| Author Scopus IDs: | 57213924436 57649843400 |
| Author Affiliations: | Sharma, S., Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee, 247 667, India Singh, U.P., Department of Chemistry, Indian Institute of Technology Roorkee, Roorkee, 247 667, India |
| Funding Details: | The authors are grateful to the BRNS , Grant No. 37018 (DAE), Mumbai, India for financial assistance. S. Sharma is thankful to UGC for fellowship. Department of Atomic Energy, Government of India, DAE; University Grants Committee, UGC; Board of Research in Nuclear Sciences, BRNS: 37018 |
| Corresponding Author: | Singh, U.P.; Department of Chemistry, India; email: udaipfcy@iitr.ac.in |
| Appears in Collections: | Journal Publications [CY] |
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